SOURCE (163A2): http://usefulchem.wikispaces.com/Exp163
  • ADD container (type=one dram screwcap vial)
  • ADD compound (common name=methanol, InChIKey=OKKJLVBELUTLKV-UHFFFAOYAX, volume=1 ml)
  • WAIT (time=1 min)
  • ADD compound (common name=furfurylamine, InChIKey=DDRPCXLAQZKBJP-UHFFFAOYAX
    volume=44.18 ul)
  • VORTEX (time=20 sec)
  • WAIT (time=8 min)
  • ADD compound (common name=phenanthrene-9-carboxaldehyde, InChIKey=QECIGCMPORCORE-UHFFFAOYAE, mass=103.1 mg)
  • VORTEX (time=20 sec)
  • SONICATE (time=5min)
  • WAIT (time= 3 min)
  • ADD compound (common name=Mandelic acid, InChIKey=IWYDHOAUDWTVEP-ZETCQYMHBP , mass=76.1 mg)
  • VORTEX (time= 20 s)
  • SONICATE (time=5min)
  • WAIT (time= 1 min)
  • ADD compound (common name=tert-butyl isocyanide, InChIKey=FAGLEPBREOXSAC-UHFFFAOYAL, volume=56.5 ul)
  • VORTEX (time=20 sec)
  • SONICATED (time=10min)
  • WAIT (time=4min)
  • TAKE PICTURE
  • WAIT (time=24 hours) time is close but not exactly what is in the log
  • TAKE PICTURE
  • Wait (time=24 hours) time is close but not exactly what is in the log - also one step missing here
  • TAKE PICTURE
Exp163A2.jpg
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